| TO-11 |
Aldehyde |
Media is GFF inside a badge. Eluant has been adjusted. |
| OSHA PV2119 Modified |
Acetic Acid |
Carbon wafer instead of charcoal in a tube. |
| L-OV (Internal Method, modified NIOSH 1500) |
Organics |
Use of co-solvents to better extract alcohols, ketones; Dual column; Use of Internal Standards; Diffusive media; Different columns from column listed. |
| OSHA 52 |
Acrolein |
Carbowax column; diffusive badge (Treated silica gel on aluminum wafer). External Calibration. Standards prepared by adding acrolein into a solution of 2-HMP and toluene, instead of spiking onto media. Extracted with 2 mL instead of 1 mL. All standard solutions and extracts stored in amber glass. |
| NIOSH 1604 |
Acrylonitrile |
Diffusive badge, benzyl alcohol co-solvent instead of acetone; Use of internal standards; dual column |
| OSHA 125 |
Metals |
All ICP metals are analyzed following OSHA 125 Modified. However, the sample prep changes depending on metals requested and collection media: Analyses which include either Silver, Antimony, Tin, Iron or Titanium are prepared using a modification of NIOSH 7303 and OSHA 206 (Hydrochloric and Nitric acids used in Hot Block digestion, final sample - matrix 20% Hydrochloric acid.) Others (MCE, PVC, Ghost wipes) are prepared using a modification of NIOSH 7082 and OSHA 121. (Nitric acid used in Hot Block digestion, final sample matrix - 5% Nitric acid.). For Non-dissolving wipes (Smear Tabs), the preparation is a modification of NIOSH 7105. (Hydrochloric (if Ag, Sb, Sn, Fe, Ti included) and Nitric acids with 30% hydrogen peroxide digested on hot plate.) ELLAP Ghost Wipes are prepared using modifications of NIOSH 9102 and NIOSH 7303 (Hydrochloric and Nitric Acids, final sample matrix – 10% HNO3, 4% HCl. |
| OSHA 188 |
Ammonia |
GFF treated media instead of carbon beads. Utilized the ISE option. |
| NIOSH 6011 |
Chlorine, Bromine |
None |
| OSHA 60 |
Amine |
Badge Media: NIT on GFF. Reverse Phase instead of normal phase. Solvent: Acetonitrile/Water. |
| OSHA 32 |
Phenols (badge) |
Badge Media: Carbon instead of silica gel. |
| NIOSH 500, 600 |
Dust |
None |
| OSHA 55 |
Super Glue |
Tenax-TA media instead of XAD-7. Media inside of diffusive monitor. |
| ASTM D5578 |
Ethylene Oxide |
Carbowax column; Badge media different carbon than the tube; Acetonitrile/Toluene Solvent (badges only) |
| NIOSH 2016 |
Formaldehyde |
DNPH on GFF instead of silica gel. Use of buffer to neutralize the extract. Methanol as eluant. |
| OSHA 64 |
Glutaraldehyde |
NPH on GFF instead of silica gel. Use of buffer to neutralize the extract. Methanol as eluant. |
| NIOSH 2532 |
Glutaraldehyde |
DNPH on GFF instead of silica gel. Use of buffer to neutralize the extract. Methanol as eluant. |
| OSHA 42, 47 |
Isocyanates |
None |
| NIOSH 7903 |
Acids |
None |
| NIOSH 6013 |
Hydrogen Sulfide |
Slightly different extraction solution. |
| NIOSH 1550 |
Hydrocarbon mixtures |
Internal Standard, Dual Column Confirmation, Diffusive media. |
| NIOSH 6014 |
Nitrogen Oxides |
Badges Only: Sampling media is treated GFF instead of instead of treated molecular sieves. |
| OSHA 214 |
Ozone |
Collection media inside a diffusive monitor instead of a cassette. Slightly different eluant. |
| NIOSH 1500 |
Hydrocarbons |
Internal Standard, Dual Column Confirmation, Diffusive media |
| OSHA 103 |
Anesthetic Gases |
Diffusive media instead of a tube when applicable. Extracted in 2 mL of toluene with internal standard calibration. Dual FID instead of just one column. |